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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7424-82-0
合成路线
（共 8 条）
7424-82-0
→
反应条件
868615-35-4
反应条件
1.1: 89 percent / CH2Cl2 / 4 h / 20 °C 2.1: 89 percent / TiCl4 / CH2Cl2 / 2 h / -78 °C 3.1: triethylamine; DMAP / CH2Cl2 / 1.5 h / 0 - 20 °C 3.2: 90 percent / DBU / toluene / 1 h / 110 °C 4.1: 70 percent / CuI / diethyl ether / 1 h / -30 °C 5.1: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C 6.1: 65 percent / Pb(OAc)4; I2 / CCl4 / 1 h / 80 °C / Irradiation View Scheme
参考文献
Drege, Emmanuelle; Morgant, Georges; Desmaele, Didier
Tetrahedron Letters, 2005 , vol. 46, # 42 p. 7263 - 7266
7424-82-0
→
反应条件
868615-50-3
反应条件
1.1: 89 percent / CH2Cl2 / 4 h / 20 °C 2.1: 89 percent / TiCl4 / CH2Cl2 / 2 h / -78 °C 3.1: triethylamine; DMAP / CH2Cl2 / 1.5 h / 0 - 20 °C 3.2: 90 percent / DBU / toluene / 1 h / 110 °C 4.1: 70 percent / CuI / diethyl ether / 1 h / -30 °C 5.1: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C View Scheme
参考文献
Drege, Emmanuelle; Morgant, Georges; Desmaele, Didier
Tetrahedron Letters, 2005 , vol. 46, # 42 p. 7263 - 7266
7424-82-0
→
反应条件
918813-45-3
反应条件
potassium hydroxide in methanol T=20°C; 16 h;
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
7424-82-0
→
反应条件
918813-46-4
反应条件
1: 97 percent / potassium hydroxide / methanol / 16 h / 20 °C 2: 84 percent / iodine; Pb(OAc)4 / CCl4 / 1 h / 80 °C / Irradiation View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
7424-82-0
→
反应条件
918813-47-5
反应条件
1: 97 percent / potassium hydroxide / methanol / 16 h / 20 °C 2: 84 percent / iodine; Pb(OAc)4 / CCl4 / 1 h / 80 °C / Irradiation 3: 86 percent / triethylamine / CH2Cl2 / 3 h / 0 °C View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
7424-82-0
→
反应条件
918813-49-7
反应条件
1: 97 percent / potassium hydroxide / methanol / 16 h / 20 °C 2: 84 percent / iodine; Pb(OAc)4 / CCl4 / 1 h / 80 °C / Irradiation 3: 65 percent / NaBH4 / ethanol / 3 h / 20 °C View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
7424-82-0
→
反应条件
918813-56-6
反应条件
1.1: 89 percent / CH2Cl2 / 4 h / 20 °C 2.1: 89 percent / TiCl4 / CH2Cl2 / 2 h / -78 °C 3.1: triethylamine; DMAP / CH2Cl2 / 1.5 h / 0 - 20 °C 3.2: 90 percent / DBU / toluene / 1 h / 110 °C 4.1: 70 percent / CuI / diethyl ether / 1 h / -30 °C 5.1: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C 6.1: 65 percent / Pb(OAc)4; I2 / CCl4 / 1 h / 80 °C / Irradiation 7.1: 70 percent / dimethylformamide / 3 h / 110 °C View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
7424-82-0
→
反应条件
918813-63-5
反应条件
1.1: 89 percent / CH2Cl2 / 4 h / 20 °C 2.1: 89 percent / TiCl4 / CH2Cl2 / 2 h / -78 °C 3.1: triethylamine; DMAP / CH2Cl2 / 1.5 h / 0 - 20 °C 3.2: 90 percent / DBU / toluene / 1 h / 110 °C 4.1: 70 percent / CuI / diethyl ether / 1 h / -30 °C 5.1: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C 6.1: 65 percent / Pb(OAc)4; I2 / CCl4 / 1 h / 80 °C / Irradiation 7.1: 70 percent / dimethylformamide / 3 h / 110 °C 8.1: 80 percent / potassium carbonate / methanol / 5 h / 20 °C View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
