1,4-双(2-羟基乙基硫代)丁烷合成路线 （共 4 条）
反应条件
thionyl chloride; diethyl ether T=15 - 20°C;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 1176
反应条件
1: 2-hydroxyethanethiol With sodium ethanolate in ethanol
2: 1,4-dibromo-butane in ethanol
1 h; Heating;
参考文献
Timperley, Christopher M.; Black, Robin M.; Bird, Michael; Holden, Ian; Mundy, Joanna L.; Read, Robert W.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 9 p. 2027 - 2046
反应条件
1: 1,2-bis thiomethyl ethane With sodium ethanolate in ethanol
2: 2-chloro-ethanol in ethanol
1 h; Heating;
参考文献
Timperley, Christopher M.; Black, Robin M.; Bird, Michael; Holden, Ian; Mundy, Joanna L.; Read, Robert W.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 9 p. 2027 - 2046
反应条件
dihydrogen peroxide in trifluoroacetic acid
1.5 h; Heating;
参考文献
Timperley, Christopher M.; Black, Robin M.; Bird, Michael; Holden, Ian; Mundy, Joanna L.; Read, Robert W.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 9 p. 2027 - 2046
