乙基(2Z)-3-(3,4-二羟基苯基)丙烯酸酯合成路线 （共 7 条）
参考文献
Freudenberg; Heel
Chemische Berichte, 1953 , vol. 86, p. 190,196
反应条件
1: 98 percent / K2CO3 / ethanol / 20 h / Heating 2: 85 percent / KOH / ethanol / 20 h / Heating 3: 95 percent / DMAP; EDCI / CH2Cl2 / 24 h / 20 °C 4: 92 percent / Pd(OAc)2; Et3N; Et3SiH / CH2Cl2 / 20 °C View Scheme
参考文献
Lamidey, Anne-Marie; Fernon, Lionel; Pouysegu, Laurent; Delattre, Charlotte; Quideau, Stephane; Pardon, Patrick
Helvetica Chimica Acta, 2002 , vol. 85, # 8 p. 2328 - 2334
反应条件
1: 98 percent / K2CO3 / ethanol / 20 h / Heating 2: 85 percent / KOH / ethanol / 20 h / Heating 3: 95 percent / DMAP; EDCI / CH2Cl2 / 24 h / 20 °C 4: 92 percent / Pd(OAc)2; Et3N; Et3SiH / CH2Cl2 / 20 °C View Scheme
参考文献
Lamidey, Anne-Marie; Fernon, Lionel; Pouysegu, Laurent; Delattre, Charlotte; Quideau, Stephane; Pardon, Patrick
Helvetica Chimica Acta, 2002 , vol. 85, # 8 p. 2328 - 2334
反应条件
1: 98 percent / K2CO3 / ethanol / 20 h / Heating 2: 85 percent / KOH / ethanol / 20 h / Heating 3: 95 percent / DMAP; EDCI / CH2Cl2 / 24 h / 20 °C 4: 92 percent / Pd(OAc)2; Et3N; Et3SiH / CH2Cl2 / 20 °C View Scheme
参考文献
Lamidey, Anne-Marie; Fernon, Lionel; Pouysegu, Laurent; Delattre, Charlotte; Quideau, Stephane; Pardon, Patrick
Helvetica Chimica Acta, 2002 , vol. 85, # 8 p. 2328 - 2334
反应条件
1: methanol. KOH 2: Hydrogenation View Scheme
参考文献
Freudenberg; Heel
Chemische Berichte, 1953 , vol. 86, p. 190,196
反应条件
potassium carbonate in ethanol
20 h; Heating;
参考文献
Lamidey, Anne-Marie; Fernon, Lionel; Pouysegu, Laurent; Delattre, Charlotte; Quideau, Stephane; Pardon, Patrick
Helvetica Chimica Acta, 2002 , vol. 85, # 8 p. 2328 - 2334
反应条件
silver carbonate in acetone; benzene
24 h; Further byproducts given;
参考文献
Antus, Sandor; Baitz-Gacs, Eszter; Bauer, Rudolf; Gottsegen, Agnes; Seligmann, Otto; Wagner, Hildebert
Liebigs Annalen der Chemie, 1989 , p. 1147 - 1152
