2,2'-[氧基二(2,1-乙二基硫代)]二-乙醇合成路线 （共 11 条）
参考文献
Woodward
Journal of the Chemical Society, 1948 , p. 37
反应条件
1: 2-hydroxyethanethiol With sodium hydroxide in ethanol
T=45°C;
2: 1-chloro-2-(2-chloroethoxy)ethane in ethanol
0.333333 h; Heating;
参考文献
Timperley, Christopher M.; Black, Robin M.; Bird, Michael; Holden, Ian; Mundy, Joanna L.; Read, Robert W.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 9 p. 2027 - 2046
反应条件
1: bis(2-mercaptoethyl)ether With sodium ethanolate in ethanol
2: 2-chloro-ethanol in ethanol
1 h; Heating;
参考文献
Timperley, Christopher M.; Black, Robin M.; Bird, Michael; Holden, Ian; Mundy, Joanna L.; Read, Robert W.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 9 p. 2027 - 2046
参考文献
Brown; Woodward
Journal of the Chemical Society, 1948 , p. 43
参考文献
Zafrani, Yossi; Goldvaser, Michael; Dagan, Shai; Feldberg, Liron; Mizrahi, Dana; Waysbort, Daniel; Gershonov, Eytan; Columbus, Ishay
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8464 - 8467
反应条件
hydrogen bromide
T=100°C;
参考文献
Woodward
Journal of the Chemical Society, 1948 , p. 37
参考文献
Woodward
Journal of the Chemical Society, 1948 , p. 37
反应条件
in tetrahydrofuran; benzene
参考文献
Bradshaw,J.S. et al.
Journal of Heterocyclic Chemistry, 1978 , vol. 15, p. 825 - 831
反应条件
in tetrahydrofuran; benzene
Heating;
参考文献
Bradshaw,J.S. et al.
Journal of Heterocyclic Chemistry, 1978 , vol. 15, p. 825 - 831
反应条件
thionyl chloride; chloroform
参考文献
Woodward
Journal of the Chemical Society, 1948 , p. 37
