1-羟基-2-甲氧基-3-甲基蒽醌合成路线 (共 4 条)
反应条件
in diethyl ether
T=20°C;
参考文献
Board of Trustees of Michigan State University
Patent: US2005/267307 A1, 2005 ;
Location in patent: Page/Page column 4, 5 ;
反应条件
1: 50 percent / AlCl3; NaCl / 4 h / 165 °C
2: 80 percent / diethyl ether / 20 °C
View Scheme
参考文献
Dhananjeyan, Mugunthu R.; Milev, Youli P.; Kron, Michael A.; Nair, Muraleedharan G.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2822 - 2830
反应条件
1: 50 percent / AlCl3; NaCl / 4 h / 165 °C
2: 80 percent / diethyl ether / 20 °C
View Scheme
参考文献
Dhananjeyan, Mugunthu R.; Milev, Youli P.; Kron, Michael A.; Nair, Muraleedharan G.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2822 - 2830
反应条件
(i), (ii) (pyrolysis), (iii) aq. HCl; Multistep reaction;
参考文献
Savard,J.; Brassard,P.
Tetrahedron Letters, 1979 , p. 4911 - 4914