2,3-双(苄氧基)苯甲酸合成路线 （共 10 条）
反应条件
1,1'-carbonyldiimidazole 1) THF, 2) THF, r.t., overnight; Yield given. Multistep reaction;
参考文献
Duhme, Annc-Kathrin; Hider, Robert Charles; Khodr, Hicham Hussein
Chemische Berichte, 1997 , vol. 130, # 7 p. 969 - 973
反应条件
1: diphenyl phosphoryl azide; triethylamine / tetrahydrofuran / 6 h / 80 °C 2: ethanol; potassium hydroxide / 18 h / Reflux 3: palladium 10 on activated carbon; hydrogen / tetrahydrofuran; methanol / 4560.31 Torr View Scheme
参考文献
Rubino, Maria Teresa; Maggi, Dariana; Laghezza, Antonio; Loiodice, Fulvio; Tortorella, Paolo
Archiv der Pharmazie, 2011 , vol. 344, # 9 p. 557 - 563
反应条件
sodium hydroxide in methanol
3 h; Reflux;
参考文献
Baramov, Todor; Keijzer, Karlijn; Irran, Elisabeth; Moesker, Eva; Baik, Mu-Hyun; Suessmuth, Roderich
Chemistry - A European Journal, 2013 , vol. 19, # 32 p. 10536 - 10542
反应条件
1: With potassium carbonate in acetone
24 h; Reflux;
2: With lithium hydroxide hydrate in methanol; water
3 h; Reflux;
3: With hydrogenchloride in methanol; water
T=0°C;
参考文献
Leydier, Antoine; Lin, Yi; Arrachart, Guilhem; Turgis, Raphael; Lecercle, Delphine; Favre-Reguillon, Alain; Taran, Frederic; Lemaire, Marc; Pellet-Rostaing, Stephane
Tetrahedron, 2012 , vol. 68, # 4 p. 1163 - 1170
反应条件
barium dihydroxide in tetrahydrofuran
T=50°C; 12 h;
参考文献
Soengas, Raquel G.; Larrosa, Marta; Balado, Miguel; Rodriguez, Jaime; Lemos, Manuel L.; Jimenez, Carlos
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 7 p. 1278 - 1287
反应条件
sodium chlorite; aminosulfonic acid in water; acetone
1 h; Ambient temperature;
参考文献
Rastetter; Erickson; Venuti
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3579 - 3590
反应条件
1: 89 percent / SOCl2
2: 99 percent / potassium carbonate / Heating
3: 100 percent / aq. barium hydroxide / tetrahydrofuran / 12 h / 50 °C
View Scheme
参考文献
Soengas, Raquel G.; Anta, Cristina; Espada, Alfonso; Nieto, Rosa M.; Larrosa, Marta; Rodriguez, Jaime; Jimenez, Carlos
Tetrahedron Letters, 2007 , vol. 48, # 17 p. 3021 - 3024
反应条件
1: K2CO3 / ethanol
2: 90 percent / NaClO2, H2NSO3H / acetone; H2O / Ambient temperature
View Scheme
参考文献
Graf, Ernest; Hosseini, Mir Wais; De Cian, Andre; Fischer, Jean
Tetrahedron Letters, 1998 , vol. 39, # 21 p. 3501 - 3504
反应条件
1: K2CO3 / ethanol
2: 90 percent / NaClO2, H2NSO3H / acetone; H2O / Ambient temperature
View Scheme
参考文献
Graf, Ernest; Hosseini, Mir Wais; De Cian, Andre; Fischer, Jean
Tetrahedron Letters, 1998 , vol. 39, # 21 p. 3501 - 3504
反应条件
1: K2CO3 / ethanol / 18 h / Heating
2: 94 percent / H2NSO3H, NaClO2 / acetone; H2O / 1 h / Ambient temperature
View Scheme
参考文献
Rastetter; Erickson; Venuti
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3579 - 3590
