2-(4-甲氧基苯基)丙-2-醇合成路线 （共 43 条）
反应条件
1: in tetrahydrofuran T=10 - 15°C; 5.5 h; Heating; 2: With water in tetrahydrofuran T=15°C; 3 h;
参考文献
DALTON CHEMICAL LABORATORIES INC.; MIKAYLO, Valeriy; PARAMANANTHAM, Subakar; AVRUTOV, Ilya; BROWN, Martyn, A.; LI, Zemin; LAZAROWYCH, Natalie
Patent: WO2010/22520 A1, 2010 ;
Location in patent: Page/Page column 9 ;
参考文献
Richardson, William H.; Stiggal-Estberg, Diana L.
Journal of the American Chemical Society, 1982 , vol. 104, # 15 p. 4173 - 4179
反应条件
in diethyl ether Heating;
参考文献
Lemiegre, Loic; Regnier, Thomas; Combret, Jean-Claude; Maddaluno, Jacques
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 373 - 377
反应条件
chloro-trimethyl-silane in tetrahydrofuran; diethyl ether T=0°C; 2 h; Yields of byproduct given;
参考文献
Rubottom, George M.; Kim, Chong-wan
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1550 - 1552
反应条件
strontium in tetrahydrofuran T=20°C; Barbier reaction; 0.5 h;
参考文献
European Journal of Organic Chemistry, , # 20 p. 4253 - 4255
反应条件
dipotassium peroxodisulfate; perchloric acid in water T=25°C; pH=1.0; 0.00833333 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 73, # 2 p. 618 - 629
参考文献
Journal of the American Chemical Society, , vol. 100, p. 3847 - 3855
反应条件
perchloric acid; sodium perchlorate in acetonitrile T=25°C; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 116, # 15 p. 6706 - 6712
反应条件
1: methyl bromide With magnesium in diethyl ether 2: 1-(4-methoxyphenyl)ethanone in diethyl ether T=20°C; Grignard reaction; 6 h; Further stages.;
参考文献
Tetrahedron Asymmetry, , vol. 18, # 12 p. 1457 - 1464
反应条件
cytochrome P450BM3 CYP102A1 monooxygenase; NADPH; bovine liver catalase in dimethyl sulfoxide T=30°C; pH=7.4; aq. bufferEnzymatic reaction;
参考文献
Chemistry - A European Journal, , vol. 14, # 35 p. 10905 - 10908
