2-氯-1-(2-羟基苯基)-1-丙酮合成路线 （共 7 条）
反应条件
water in 1,4-dioxane
12 h; Ambient temperature;
参考文献
Silverman, Richard B.
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3910 - 3915
反应条件
1: 1.) triethylamine, 2.) Cl2 / 1) THF; 2) ice-cooling, 30 min
2: 76 percent / H2O / dioxane / 12 h / Ambient temperature
View Scheme
参考文献
Silverman, Richard B.
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3910 - 3915
反应条件
1: 33 h / 120 - 130 °C
2: 76 percent / H2O / dioxane / 12 h / Ambient temperature
View Scheme
参考文献
Silverman, Richard B.
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3910 - 3915
反应条件
1: 40 percent / NaH / benzene / 72 h / Heating
2: 1.) triethylamine, 2.) Cl2 / 1) THF; 2) ice-cooling, 30 min
3: 76 percent / H2O / dioxane / 12 h / Ambient temperature
View Scheme
参考文献
Silverman, Richard B.
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3910 - 3915
反应条件
aluminium trichloride
zuletzt bei 110grad;
参考文献
v. Auwers; Poetz; Noll
Justus Liebigs Annalen der Chemie, 1938 , vol. 535, p. 219,248
反应条件
1: 135 °C
2: AlCl3 / zuletzt bei 110grad
View Scheme
参考文献
v. Auwers; Poetz; Noll
Justus Liebigs Annalen der Chemie, 1938 , vol. 535, p. 219,248
反应条件
iron(III) chloride
T=170°C; 24 h; MechanismProduct distribution;
参考文献
Martin, Robert; Lafrance, Jean Ronald; Demerseman, Pierre
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 7 p. 539 - 548
