N-苄氧羰基-L-色氨酸合成路线 （共 39 条）
反应条件
triethylamine in water Ambient temperature;
参考文献
Azuse; Tamura; Kinomura; Okai; Kouge; Hamatsu; Koizumi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3103 - 3108
反应条件
1: With water; lithium hydroxide hydrate in tetrahydrofuran T=20°C; 3 h; 2: With hydrogenchloride in water pH=5;
参考文献
European Journal of Organic Chemistry, , # 1 p. 67 - 73
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide; Dec-L-His in acetonitrile T=25°C; 0.02M phosphate buffer, pH=7.3; other catalysts; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 607 - 612
反应条件
1.1: triethylamine / dichloromethane / 2 h / 20 °C 2.1: water; lithium hydroxide hydrate / tetrahydrofuran / 3 h / 20 °C 2.2: pH 5 View Scheme
参考文献
European Journal of Organic Chemistry, , # 1 p. 67 - 73
反应条件
1: 53 percent / 8 h / Ambient temperature 2: 95 percent / aq. NaOH / dioxane / 1 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 11 p. 958 - 960
反应条件
γ-cyclodextrin in acetonitrile T=25°C; pH=9.5; Kinetics; Further Variations:Reagents;
参考文献
Chemical and pharmaceutical bulletin, , vol. 50, # 9 p. 1283 - 1285
反应条件
resolved on CSP cellulose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Chemistry Letters, , p. 1125 - 1128
反应条件
1: methyl chloroformate 2: hydrogen / 10 percent Pd/C 3: MeOH; Et3N / Heating View Scheme
参考文献
Fukui, Yoshikazu; Somei, Masanori
Heterocycles, 2001 , vol. 55, # 11 p. 2055 - 2057
反应条件
1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine 2: hydrogen / methanol / 50 °C View Scheme
参考文献
Hudecova, Jana; Hornicek, Jan; Budesinsky, Milos; Sebestik, Jaroslav; Safarik, Martin; Zhang, Ge; Keiderling, Timothy A.; Bour, Petr
ChemPhysChem, 2012 , vol. 13, # 11 p. 2748 - 2760
反应条件
1: NMM; IBCF; 28percent aq. NH3 / 1,2-dimethoxy-ethane 2: aq. HCl; H2 / 10percent Pd/C / dimethylformamide / 24 h View Scheme
参考文献
Guerlavais, Vincent; Boeglin, Damien; Mousseaux, Delphine; Oiry, Catherine; Heitz, Annie; Deghenghi, Romano; Locatelli, Vittorio; Torsello, Antonio; Ghe, Corrado; Catapano, Filomena; Muccioli, Giampiero; Galleyrand, Jean-Claude; Fehrentz, Jean-Alain; Martinez, Jean
Journal of Medicinal Chemistry, 2003 , vol. 46, # 7 p. 1191 - 1203
