N-苄氧羰基-L-色氨酸合成路线 （共 39 条）
反应条件
potassium carbonate in acetonitrile
24 h; Heating;
参考文献
Yoshino, Tomonori; Togo, Hideo
Synlett, 2005 , # 3 art. no. U29304ST, p. 517 - 519
反应条件
potassium hydrogencarbonate in N,N-dimethyl-formamide
T=0 - 20°C;
参考文献
Yokokawa, Fumiaki; Sugiyama, Hideyuki; Aoyama, Toyohiko; Shioiri, Takayuki
Synthesis, 2004 , # 9 p. 1476 - 1480
反应条件
potassium hydroxide in diethyl ether; ethanol; dichloromethane; water
参考文献
Ekhato, I. Victor; Huang, Yun
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 12 p. 1019 - 1038
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Xiao, Jian; Xu, Feng-Xia; Lu, Yun-Peng; Loh, Teck-Peng
Organic Letters, 2010 , vol. 12, # 6 p. 1220 - 1223
反应条件
caesium carbonate in N,N-dimethyl-formamide
参考文献
Ekhato, I. Victor; Huang, Yun
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 12 p. 1019 - 1038
反应条件
dicyclohexyl-carbodiimide in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Dubowchik, Gene M.; Firestone, Raymond A.
Bioorganic & Medicinal Chemistry Letters, 1998 , vol. 8, # 23 p. 3343 - 3346
反应条件
pyridine in acetonitrile
参考文献
Griffin, Martin; Mongeot, Alexandre; Collighan, Russell; Saint, Robert E.; Jones, Richard A.; Coutts, Ian G.C.; Rathbone, Daniel L.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 20 p. 5559 - 5562
反应条件
triethylamine; isobutyl chloroformate in tetrahydrofuran
T=-15 - 22°C; 0.5 h;
参考文献
Westerhuis, L. W.; Tesser, G. I.; Nivard, R. J. F.
Recueil: Journal of the Royal Netherlands Chemical Society, 1980 , vol. 99, # 12 p. 400 - 403
反应条件
1.1: SOCl2 / tetrahydrofuran / 0.33 h / 40 - 50 °C
1.2: 95 percent / tetrahydrofuran / 2 h / 20 °C
2.1: 85 percent / Et3N / acetonitrile; H2O / 1 h / 20 °C
View Scheme
参考文献
Moss, Robert A.; Taguchi, Takayuki; Bizzigotti, George O.
Tetrahedron Letters, 1982 , vol. 23, # 19 p. 1985 - 1988
