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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
反-5-癸烯
合成路线
（共 88 条）
109-72-8
正丁基锂
+
85260-47-5
→
反应条件
7433-56-9
反-5-癸烯
+
57266-88-3
+
57266-87-2
反应条件
in diethyl ether -78 deg C -> RT; Yields of byproduct given;
参考文献
Ukaji, Yutaka; Yoshida, Akifumi; Fujisawa, Tamotsu
Chemistry Letters, 1990 , p. 157 - 160
94616-73-6
+
85260-47-5
→
反应条件
7433-56-9
反-5-癸烯
+
57266-88-3
+
57266-87-2
反应条件
in diethyl ether -78 deg C -> RT; Yields of byproduct given;
参考文献
Ukaji, Yutaka; Yoshida, Akifumi; Fujisawa, Tamotsu
Chemistry Letters, 1990 , p. 157 - 160
89609-03-0
→
反应条件
7433-56-9
反-5-癸烯
反应条件
in N,N-dimethyl-formamide electrochemical dehalogenation at mercury pool cathode at constant potential; Product distribution;
参考文献
Zavada, Jiri; Krupicka, Josef; Kocian, Oldrich; Pankova, Magdalena
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 12 p. 3552 - 3558
89608-99-1
→
反应条件
7433-56-9
反-5-癸烯
反应条件
in N,N-dimethyl-formamide electrochemical dehalogenation at mercury pool cathode at constant potential; Product distribution;
参考文献
Zavada, Jiri; Krupicka, Josef; Kocian, Oldrich; Pankova, Magdalena
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 12 p. 3552 - 3558
89609-05-2
→
反应条件
7433-56-9
反-5-癸烯
反应条件
in N,N-dimethyl-formamide electrochemical dehalogenation at mercury pool cathode at constant potential; Product distribution;
参考文献
Zavada, Jiri; Krupicka, Josef; Kocian, Oldrich; Pankova, Magdalena
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 12 p. 3552 - 3558
109-72-8
正丁基锂
+
37490-22-5
→
反应条件
7433-56-9
反-5-癸烯
反应条件
palladium diacetate; triethylamine 1.) THF, hexane, 0 deg C, 30 min, 2.) THF, hexane, overnight; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 6 p. 1670 - 1676
109-72-8
正丁基锂
+
152841-67-3
→
反应条件
7433-78-5
顺式-5-癸烯
+
7433-56-9
反-5-癸烯
反应条件
potassium hydride 1.) ether, -78 deg C, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 34, # 23 p. 3695 - 3698
41929-38-8
→
反应条件
7433-56-9
反-5-癸烯
+
30651-68-4
反应条件
palladium diacetate; n-butyllithium; triethylamine 1.) THF, -78 deg C, 2.) THF, RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 6 p. 1670 - 1676
693-04-9
氯丁基镁
→
反应条件
7433-78-5
顺式-5-癸烯
+
7433-56-9
反-5-癸烯
反应条件
potassium hydride 1.) THF, -78 deg C, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 34, # 23 p. 3695 - 3698
693-04-9
氯丁基镁
+
152841-67-3
→
反应条件
7433-78-5
顺式-5-癸烯
+
7433-56-9
反-5-癸烯
反应条件
potassium hydride 1.) ether, -78 deg C, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 34, # 23 p. 3695 - 3698
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