5-氨基乙基-6-氟-苯并[1,3]二氧代合成路线 (共 3 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Moreau, Anne; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre; Lebrun, Stephane
Tetrahedron, 2004 , vol. 60, # 29 p. 6169 - 6176
反应条件
1: 71 percent / cesium carbonate / dimethylformamide / 3 h / 110 °C
2: 67 percent / AcONH4 / 5 h / Heating
3: 51 percent / LiAlH4 / tetrahydrofuran
View Scheme
参考文献
Moreau, Anne; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre; Lebrun, Stephane
Tetrahedron, 2004 , vol. 60, # 29 p. 6169 - 6176
反应条件
1: 67 percent / AcONH4 / 5 h / Heating
2: 51 percent / LiAlH4 / tetrahydrofuran
View Scheme
参考文献
Moreau, Anne; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre; Lebrun, Stephane
Tetrahedron, 2004 , vol. 60, # 29 p. 6169 - 6176