(2,2-二溴乙烯基)苯合成路线 (共 99 条)
反应条件
copper(l) iodide; 8-hydroxy-quinoline; potassium carbonate in N,N-dimethyl-formamide
T=110°C; 24 h; Inert atmosphere;
参考文献
Yan, Hong; Lu, Linhua; Sun, Peng; Zhu, Yan; Yang, Hailong; Liu, Defu; Rong, Guangwei; Mao, Jincheng
RSC Advances, 2013 , vol. 3, # 2 p. 377 - 381
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=90°C; 2 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
Organic Letters, 2010 , vol. 12, # 9 p. 2048 - 2051
反应条件
copper(l) iodide; 8-hydroxy-quinoline; potassium carbonate in N,N-dimethyl-formamide
T=110°C; 24 h; Inert atmosphere; ConcentrationReagent/catalystSolventTemperatureTime;
参考文献
Yan, Hong; Lu, Linhua; Sun, Peng; Zhu, Yan; Yang, Hailong; Liu, Defu; Rong, Guangwei; Mao, Jincheng
RSC Advances, 2013 , vol. 3, # 2 p. 377 - 381
反应条件
aluminum oxide; potassium fluoride; copper(l) iodide; triphenylphosphine; nickel
0.05 h; microwave irradiation;
参考文献
Yan, Jincan; Wang, Zhiyuan; Wang, Lei
Journal of Chemical Research, 2004 , # 1 p. 71 - 73
反应条件
caesium carbonate in toluene
T=120°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Wang, Yulei; Gan, Jiepeng; Liu, Liu; Yuan, Hang; Gao, Yuxing; Liu, Yan; Zhao, Yufen
Journal of Organic Chemistry, 2014 , vol. 79, # 8 p. 3678 - 3683
反应条件
water in N,N-dimethyl-formamide
T=100°C; 16 h;
参考文献
Shen, Wang; Kunzer, Aaron
Organic letters, 2002 , vol. 4, # 8 p. 1315 - 1317
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide
T=120°C; 48 h;
参考文献
Liu, Guoping; Cong, Xuefeng; He, Jiaheng; Luo, Shunzhong; Wu, Di; Lan, Jingbo
Journal of Chemical Research, 2012 , vol. 36, # 12 p. 687 - 690
反应条件
potassium fluoride in N,N-dimethyl-formamide
T=130°C; 12 h; Inert atmosphere; Reagent/catalystConcentrationSolventTemperatureTime; regioselective reaction;
参考文献
Liu, Guoping; Cong, Xuefeng; He, Jiaheng; Luo, Shunzhong; Wu, Di; Lan, Jingbo
Journal of Chemical Research, 2012 , vol. 36, # 12 p. 687 - 690
反应条件
caesium carbonate in dimethyl sulfoxide
T=100°C; Inert atmosphere;
参考文献
Ni, Zhangqin; Wang, Sichang; Mao, Hui; Pan, Yuanjiang
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3907 - 3910
反应条件
in dimethyl sulfoxide
T=35 - 40°C; 7 h; Irradiation1.) var. of reaction time; 2.) var. of condition of irradiation; 3.) other PhC<*>CQ substrates with different alkyl or aryl mercury chlorides; 4.) var. concentration, radiation source.; Product distributionMechanism;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha
Tetrahedron Letters, 1986 , vol. 27, # 30 p. 3479 - 3482