2,3,4,6,7,8-六氢-[1,3,2]氧氮杂膦咛并[2,3-b][1,3,2]氧氮杂膦咛合成路线 （共 2 条）
→
74378-80-62,3,4,6,7,8-六氢-[1,3,2]氧氮杂膦咛并[2,3-b][1,3,2]氧氮杂膦咛
反应条件
tris-(dimethylamino)-phosphine in toluene
48 h; Heating;
参考文献
Denney,D.B.; Denney,D.Z.; Hammond,P.J.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5073
→
74378-80-62,3,4,6,7,8-六氢-[1,3,2]氧氮杂膦咛并[2,3-b][1,3,2]氧氮杂膦咛
反应条件
1: 37 percent / LiAlH4 / diethyl ether / 1.) room temperature, 1 h, 2.) reflux, 24 h
2: 16 percent / hexamethylphosphorous triamide / toluene / 48 h / Heating
View Scheme
参考文献
Denney,D.B.; Denney,D.Z.; Hammond,P.J.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5073
