反应条件
in neat (no solvent, solid phase) byproducts: LiCl, N2; Sonication; grinding in agate mortar; sealing in glass ampoule under vac.; sonicating (ultrasonic gun), 10 min; heating, 400°C, 5-10 min; sublimation of LiCl onto reactor walls; cooling to room temp.; open of ampoule under N2; trituration with THF, 10h; pptn.; washing with water or THF;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , # 16 p. 2435 - 2438
