反应条件
in solid powders mixed, set in alumina boat and annealed in furnacen (heat at 6 °C/min to 1000 °C, hold for 1 h, cooled at 3°C/min),N2 pressure 0.10 MPa, gas flow 100 sccm, soot centrifuged at 8000 rpm f or 2 min, liquid removed;
参考文献
Solid State Communications, , vol. 136, # 6 p. 342 - 345
