Klemm, W.; Tilk, W.; Muellenheim, S. v.
Z. Anorg. Chem., 1928 , vol. 176, p. 1 - 22
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Gmelin Handbook: Cd: SVol., 10.4, page 457 - 462
in hexane byproducts: hexamethylbenzene; iron atoms and 2-butyne were cocondenced with pentane under high vac. conditions on the liquid nitrogen cooled walls, then warming to room temp.; evapn., gradient vacuum sublimation;
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Journal of Organometallic Chemistry, , vol. 249, # 1 p. 195 - 204
in neat (no solvent) mixt. of CaO, CuO, Fe, and S (3:2:2:2 ratio) ground, pelletized, sealed in evacuated quartz tube and annealed twice at 750°C for 48 h with intermediate re-grinding and re-pelletizing; not isolated, detn. by XRD;
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Charkin; Sadakov; Omel'Yanovskii; Kazakov
Materials Research Bulletin, 2010 , vol. 45, # 12 p. 2012 - 2016
