in solid pressing SiC and Fe (100 MPa), heating at 850-1600°C for 1 h (N2 or Ar); DTA, X-ray diffraction;
参考文献
Journal of the American Ceramic Society, , vol. 79, # 8 p. 2017 - 2026
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反应条件
in neat (no solvent) mixt. in carbon crucible fusion at 1250-1300°C for 1 h in muffler, air cooling; tubelene carbon inclusions identification using X-ray emission spectroscopy;
in solid matrix Nd:YAG laser focused onto metal target (5-10 mJ/pulse), Fe atoms were codeposited with S(x)/Ar mixt. (microwave discharge in Ar seeded with S vapor) onto CsI window cooled to 7 K, annealing to 40 K; IR spect. monitoring, not isolated;
参考文献
Binyong, Liang; Xuefeng, Wang; Lester, Andrews
Journal of Physical Chemistry A, 2009 , vol. 113, # 18 p. 5375 - 5384
