in tetrahydrofuran; toluene T=20°C; 4 h; Inert atmosphere;
参考文献
Fecker, Ann Christin; Gloeckner, Andreas; Daniliuc, Constantin G.; Freytag, Matthias; Jones, Peter G.; Walter, Marc D.
Organometallics, 2013 , vol. 32, # 3 p. 874 - 884
hydrogenchloride in formamide Electrolysis; from a soln. of 0.5g FeCl3 and 1g AlCl3 in 30 cml formamide acidified with gaseous HCl; room temp., 1.5 A/(dm*dm), Al-anode, Cu-cathode;;
sodium perchlorate in water Electrochem. Process; prepn. by electrodeposition from aq. FeCl3 soln. (0.10 mM) and 0.1 M NaClO4 (as electrolyte) in three-electrode cell on H-terminated Si substrate potentiostatically by amperometry at const. potential of -0.8 V; Si substrate removed from cell; rinsed (water); dried in N2;
sodium perchlorate in water Electrochem. Process; prepn. by electrodeposition from aq. FeCl3 soln. (10-20 mM) and 0.1 M NaClO4 (as electrolyte) in three-electrode cell on H-terminated Si substrate potentiostatically by amperometry at const. potential of -0.8 V; Si substrate removed from cell; rinsed (water); dried in N2;
octadecanoic acid in mineral oil heating of mixt. of mineral oil, Fe2(CO)9 and stearic acid at 573 K under Ar flow for 30 min; cooling at the velocity of 0.074 K/s to 314 K;
参考文献
Journal of Magnetism and Magnetic Materials, , vol. 283, # 2-3 p. 335 - 343
