lithium in neat (no solvent) reduction at 1000K, under He, Mo-vessel;;
参考文献
Stites, J. G.; Salutsky, M. L.; Stone, B. D.
Journal of the American Chemical Society, 1955 , vol. 77, p. 237 - 240
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Gmelin Handbook: Sc: MVol.C3, 6.2.5.3.1.8.2, page 164 - 164
Mg or Ca in neat (no solvent) booster: I2, addn. of o.5mol dry I2 or 0.3mol I2 and 0.0625mol KClO4 per 1mol LaCl3, CaO-coated bomb; decrease of react. temp. to 850°C on addn. of 20mol-percent KCl (flux);;
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Gmelin Handbook: Sc: MVol.B2, 2.1.4, page 210 - 211
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Keller, W. H.; Ericson, R. P.; Hach, C.
C. A., TID-5212 (1955) 32/6 1956 , p. 7698
potassium in neat (no solvent) passing K-vapor over LaBr3 in vac.;;
参考文献
Gmelin Handbook: Sc: MVol.B2, 2.1.4, page 210 - 211
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Power, W. H.; Fox, G. L.; Otto, J. B.
N. S. A., MLM-995 (1954) 1/38 1956 , vol. 10, p. 2979
Gmelin Handbook: Sc: MVol.B2, 2.4, page 233 - 234
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Foster, K. W.; Pish, G.; Schamp, H. W.; Goode, J. M.; Eyles, T. E.
N. S. A., MLM-686 (1952), S. 1/29 1953 , vol. 7, p. 2810
NaF; LiF in melt byproducts: NaLaF4, LiLaF4; heating of LaF3 and Zr in molten mixt. of 39 mol percent NaF and 61 mol percent LiF at 465 - 625°C; monitoring by differential thermal XRD and IR;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 48, # 10 p. 1454 - 1458
in ethanol Electrolysis; 20g LaCl3*H2O in 100ml ethanol, Hg cathode, 20V, current density 0.02A/cm**2, 30h, formation of an amalgame with 2.5-3 wt.-percent La, washing with ethanol and ether, generation of La by decompn.;;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 211, p. 237 - 240
