in solid matrix condensation of a stream of Li-atoms with CBr4 in an Ar-matrix at 15K on CsI (concn. Ar:CBr4 = 400-600, Li:CBr4 = 0.5-3);; determination by IR;;
参考文献
Andrews; Carver
Journal of Chemical Physics, 1968 , vol. 49, p. 896,897
Kochkanyan, R. O.; Bondarenko, A. V.; Khripunov, S. V.; Zaritovskii, A. N.; Suikov, S. Yu.
Russian Journal of General Chemistry, 1995 , vol. 65, p. 1085 - 1086
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Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 1831 - 1838
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Gmelin Handbook: Bi: Org.Verb., 1.3.3.2.4.3, page 72 - 78
in THF-d8 (tetrahydrofuran-d8) byproducts: LiCl; Sonication; Et3SnCl(0.00022 mol) and finely cut lithium(0.00053 mol) under dry Ar placed in an NMR tube and 0.5 mL anhydrous THF-d8 added; mixt. sonicated for 10 h; not isolated; detn. by NMR;
参考文献
Chugunov; Troitskii; Nosov; Egorov; Nefedov
Russian Chemical Bulletin, 2004 , vol. 53, # 10 p. 2327 - 2329
