sodium chloride in diethyl ether; water at 30°C; pouring the reaction mixture into ice-cold satd. aq. NaCl soln.; extrn. with ether; addn. of xylene and removing the ether;
参考文献
Vanderberg, J. T.; Moore, C. E.; Cassaretto, F. P.; Posvic, H.
Analytica Chimica Acta, 1969 , vol. 44, p. 175 - 183
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Gmelin Handbook: B: B-Verb.8, 11.2.3, page 167 - 173
in diethyl ether a Grignard soln. (prepd. from MeI and Mg in Et2O) is added to the suspn. of InCl3 in ether and refluxed for 3 h; distn. of excess of Et2O at atm. pressure affords Me3In*Et2O; repeated distn. of the etherate at room temp. in vac. affords InMe3;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 7 - 12
