in tetrahydrofuran addition of a solution of C2H4Br2 in THF drop by drop to a mixture of Mg and C6F6/THF (mol ratio C2H4Br2/C6F6 = 2/1) within 0.75 hours, cooling with ice water;;
参考文献
Respes et al.
Journal of Organometallic Chemistry, 1969 , vol. 19, p. 191
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
in tetrahydrofuran addition of a solution of C2H5Br in THF drop by drop to a mixture of Mg and C6F6/THF (mol ratio C2H5Br/C6F6 = 1/1) within 0.75 hours, cooling with ice water;;
参考文献
Respes et al.
Journal of Organometallic Chemistry, 1969 , vol. 19, p. 191
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
in tetrahydrofuran addition of C6H5Br to a suspension of Mg in THF (condensation of Mg- and THF-vapour at -196°C) at -30°C, 0.75 hours;;
参考文献
Clabunde, K. J.; Efner, H. F.; Satek, L.; Donley, W.
Journal of Organometallic Chemistry, 1974 , vol. 71, p. 309 - 313
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
in tetrahydrofuran reaction of Mg shavings in presence of I2 under reflux, 1 hour;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
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Imperial Smelting Corp.
Patent: GB1047318 , 1966 ;
C. A., 1967 , vol. 66, p. 18585
in diethyl ether addition of ether drop by drop to a suspension of SiCl4, Mg and C6F5Br, 12 hours;; not isolated;;
参考文献
Whittingham, A.; Jarvie, A. W. P.
Journal of Organometallic Chemistry, 1968 , vol. 13, p. 125 - 129
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
in diethyl ether addition of ether drop by drop to a suspension of (C2H5O)4Si, Mg and C6F5Br, 18 hours;; not isolated;;
参考文献
Whittingham, A.; Jarvie, A. W. P.
Journal of Organometallic Chemistry, 1968 , vol. 13, p. 125 - 129
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
