in neat (no solvent) inert condition; addn. of I2 to mixt. of Mg and Ga, heating in vac. (150°C), chilling, addn. of EtI (50 - 70°C, 1 h), heating (90 °C, 4 h); distillation;
参考文献
Zakharkin; Gavrilenko
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 7 p. 1243 - 1247
nitrogen oxidous in gaseous matrix byproducts: N2; dc discharge (potential 1.5 kV, current 50 mA) of a mixt. of hot Mg vapor, N2O and Ar, react. temp. 900 K, press. 3 Pa, color of emission changed from weak purple to green after evapn. of Mg; detection by IR spectroscopy;
参考文献
Civish, Svatopluk; Hedderich, Hartmut G.; Blom, Cornelius E.
Chemical Physics Letters, 1991 , vol. 176, p. 489 - 494
