Bryant, E. G.
Chem. News J. Ind. Sci., 1899 , vol. 79, p. 76 - 76
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Seubert, K.; Schmidt, A.
Liebigs Annalen der Chemie, 1892 , vol. 267, p. 226 - 236
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Gmelin Handbook: Mg: MVol.A2, 46, page 318 - 320
in ammonia Electrolysis; at boiling point of solvent, in not aquos soln.; with Hg-cathode,alkali-earth metal anode, Na-amalgam precipitated on the cathode;
in neat (no solvent) (Ar); stoich. mixt. of elements and NaN3 sealed in cleaned Nb ampoule, arc-welded ampoule enclosed in evac. silica tube, heated within 24 h to 800 or 1000°C, kept at this temp. for 3 d, cooled to room temp. infurnace; detn. by XRD;
参考文献
Reckeweg, Olaf; Lind, Cora; Simon, Arndt; Disalvo, Francis J.
Journal of Alloys and Compounds, 2004 , vol. 384, # 1-2 p. 98 - 105
