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in methanol Electrochem. Process; anodic oxidation of Mo in MeOH in the presence of LiCl (110 V, 12 h); concn., pptn. on cooling to 0°C, decantation, washing (cold MeoH), extn. (50°C hot hexane), evapn. (vac.), recrystn. of the residue after extn. from a min. amt. MeOH and cautious evapn. in vac.; elem. anal.;
参考文献
Kessler, Vadim G.; Panov, Andrei N.; Turova, Nataliya Ya.; Starikova, Zoya A.; Yanovsky, Alexandr I.; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1998 , # 1 p. 21 - 30
