反应条件
in neat (no solvent, solid phase) High Pressure; MoO3, KBH4 was mixed, CCl4 was added, placed in autoclave under Ar, heated to 300°C, kept for 4 h, cooled to room temp.; passivated by O2/N2 for 2 h, dissolved in water, washed, filtered, exchaned with acetone for several time, dried at room temp.;
参考文献
Journal of Solid State Chemistry, , vol. 170, # 1 p. 135 - 141
