反应条件
in ethylene glycol dimethyl ether; dichloromethane
under N2 soln. (Cp(PPh3)2Ru)2(μ-C4) in CH2Cl2 was treated dropwise with soln. AgPF6 in 1,2-dimethoxyethane; Ag was filtered off, solvent was evapord. from filtrate, residue was taken up in small amt. CH2Cl2 and filtered into rapidly stirred Et2O; elem. anal.;
参考文献
Bruce, Michael I.; Low, Paul J.; Costuas, Karine; Halet, Jean-Francois; Best, Stephen P.; Heath, Graham A.
Journal of the American Chemical Society, 2000 , vol. 122, # 9 p. 1949 - 1962