反应条件
in dichloromethane
addn. of AgBF4*0.5C4H8O2 to soln. of complex in dried and distilled solvent, molar ratio of educts: AgBF4/complex=2/1, 2h, darkness, room temp., pptd. Ag filtered off, solvent removed at reduced press.; product recrystd. from dichloromethane/pentane, reaction detected by IR;
参考文献
Callan, Brian; Manning, A. R.; Stephens, F. S.
Journal of Organometallic Chemistry, 1987 , vol. 331, # 3 p. 357 - 378