in neat (no solvent)
thermic decomposition, further products;;
参考文献
Oza, T. M.; Thaker, R. H.
Journal of the American Chemical Society, 1955 , vol. 77, p. 4976 - 4980
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Gmelin Handbook: Ag: MVol.B1, 4.21.2.6, page 188 - 188
hexan-1-ol in further solvent(s)
byproducts: CH3(CH2)4CHO; fatty acid silver salt added to 1-hexanol; the suspension stirred and heated up to 413 K under MW irradiation within 2 min under N2 atmosphere; maintained for 5 min at 413 K (or 40 min at 383 K, or 1 min at 430 K) under repeated on-off MW irradiation; suspension cooled down by an air blower;
hexan-1-ol in further solvent(s)
byproducts: CH3(CH2)4CHO; fatty acid silver salt added to 1-hexanol; the suspension stirred and heated up to 413 K under MW irradiation within 2 min under N2 atmosphere; maintained for 5 min at 413 K (or 40 min at 383 K, or 1 min at 430 K) under repeated on-off MW irradiation; suspension cooled down by an air blower;
formaldehyde in water
Irradiation (UV/VIS); trisodim citrate (0.1-1.5 M)/formaldehyde (1.0-1.5 M) added to aq. soln.of AgNO3 (up to 0.1 M); irradiated under microwave (2.45 GHz) irradiati on at 650 W for 1 min; monitored by X-ray diffraction and scanning electron microscopy;
参考文献
Yamamoto, Tetsushi; Yin, Hengbo; Wada, Yuji; Kitamura, Takayuki; Sakata, Takao; Mori, Hirotaro; Yanagida, Shozo
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 4 p. 757 - 761
hexan-1-ol in further solvent(s)
byproducts: CH3(CH2)4CHO; fatty acid silver salt added to 1-hexanol; the suspension stirred and heated up to 413 K under MW irradiation within 2 min under N2 atmosphere; maintained for 5 min at 413 K (or 40 min at 383 K, or 1 min at 430 K) under repeated on-off MW irradiation; suspension cooled down by an air blower;
hexan-1-ol in further solvent(s)
byproducts: CH3(CH2)4CHO; fatty acid silver salt added to 1-hexanol; the suspension stirred and heated up to 413 K under MW irradiation within 2 min under N2 atmosphere; maintained for 5 min at 413 K (or 40 min at 383 K, or 1 min at 430 K) under repeated on-off MW irradiation; suspension cooled down by an air blower;
