in tetrahydrofuran
byproducts: P(C6H4CH2NMe2)3; Irradiation (UV/VIS); in light in a few min; pptn of Ag, filtered, part of solvent evapd., crystn. at -30 °C;
参考文献
Leschke; Rheinwald; Lang
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 11 p. 2470 - 2477
→
反应条件
O2 in neat (no solvent, solid phase)
Bi2O3, Ag2O, TiO2 mixed, homogenized in EtOH, fired in O2 flow at 10°C/min to 900°C for 12 h; monitored by XRD;
参考文献
Hu, Xing; Skapin, Sreco D.; Suvorov, Danilo
Journal of the American Ceramic Society, 2007 , vol. 90, # 8 p. 2363 - 2366
in further solvent(s)
other Radiation; Ag nanoparticles produced by accelerated electron beam irradiation of soln. of Ag(Tf2N) in 1-butyl-3-methylimidazolium bis((trifluoromethyl)sulfonyl)amide at room temp.; UV/Vis spectroscopy, TEM;
in pyridine
from 10percent. pyridine soln. of AgCl with As between 8 days;;
参考文献
Kahlenberg, L.; Steinle, J. V.
Trans. Am. electrochem. Soc., 1923 , vol. 44, p. 493 - 516
Full Text Show Details
Gmelin Handbook: As: MVol., 51, page 181 - 184