反应条件
in diethyl ether; acetonitrile
byproducts: Me3SiF; (N2 or Ar); addn. of Et2O soln. of Me3SiC2F3 to EtCn suspn. of AgF, stirred (1 h, RT), Removal of Me3Sif in vac., addn. of Te, stirred (18 h, RT); pptn. of Ag as solid, volatiles condensed in vac at -196 °C in Schlenk tube, Te(C2F3)2 not isolated, identified via NMR;
参考文献
Naumann, Dieter; Tyrra, Wieland; Von Foullon, Alexander; Pantenburg, Ingo
Zeitschrift fur Anorganische und Allgemeine Chemie, 2009 , vol. 635, # 6-7 p. 862 - 868