反应条件
in sodium hydroxide slow addition of Na-amalgam (16 g Na + 2500 g Hg) to a cold solution of 20 g NaNO2 in aq. NaOH (10 g NaOH, 100 ml H2O) under stirring, neutralisation of the solution with HNO3 and addition of a solution of AgNO3 in H2O;; precipitation from ice cold HNO3;;
参考文献
Abel, E.; Orlicek, A.; Proisl, J.
Monatshefte fuer Chemie, 1938 , vol. 72, p. 1 - 21
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Gmelin Handbook: Ag: MVol.B1, 4.11.1, page 171 - 171
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Brauer, G.
Handbuch der praeparativen anorganischen Chemie, Stuttgart 1954, S. 375/6