Holt, W.; Sims, W. E.
Journal of the Chemical Society, 1804 , vol. 65, p. 440 - 443
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Gmelin Handbook: N: MVol.3, 2.5.2, page 722 - 725
in neat (no solvent) equilibrium reaction at higher temperatures;;
参考文献
Lorenz, R.; Winzer, R.
Z. Anorg. Chem., 1929 , vol. 181, p. 193 - 202
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Rinck, E.
Annales de Chimie (Cachan, France), 1932 , vol. 18, # 10 p. 395 - 531
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Gmelin Handbook: Ca: MVol.B2, 80, page 448 - 451
in neat (no solvent) shaking of Na, CaCl2 and NaCl in a closed supremax-tube for 30 min at 500-810°C until equilibrium; heating for 15 min at the same temperature; chilling; examination of the equilibrium;; seperation of the saltfree metal- and the saltphase under ether;;
参考文献
Lorenz, R.; Winzer, R.
Z. Anorg. Chem., 1929 , vol. 181, p. 193 - 202
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Gmelin Handbook: Ca: MVol.B2, 80, page 448 - 451
in neat (no solvent) byproducts: acetone, NaCl; addn. of Na to carbinol (room temp.), heating to 70°C (5 h), dropwise addn. of Bu2SnCl2 (as soln. in carbinol); distn. (reduced pressure);
参考文献
Tagliavini et al.
Inorganica Chimica Acta, 1978 , vol. 26, p. L41