反应条件
in ethanol; benzene byproducts: Na(CH3C(O)CHC(O)CH3); N2 atmosphere; addn. of soln. of Sn(acac)2 in C6H6 to soln. of Na in EtOH (Sn : Na = 1 : 2, stirring, room temp.), stirring (0.5 h; pptn.); filtration, washing (MeOH, benzene), drying (vac.); elem. anal.;
参考文献
Wakeshima, Ikuko; Suzuki, Toshitaka; Takemoto, Akihiko; Kijima, Ichiro
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1997 , vol. 27, # 5 p. 787 - 796
