反应条件
in ammonia
byproducts: C5H4N(OPO(OC2H5)2); NH3 (liquid); Irradiation (UV/VIS); (inert atm.); addn. of sodium to soln. of 2.2 or 1 equiv. of tin compd. in liquid ammonia, addn. of 1 equiv. of pyridine deriv., stirring with irradiation for 10 or 60 min; quenching with methyl iodide, adn. of diethyl ether, evapn. of ammonia, treating with water, extn. (diethyl ether), washing with water and brine, drying over MgSO4, filtration, evapn., chromy. (silica gel, hexane/ethyl acetate (6:4)), elem. anal.;
参考文献
Silbestri, Gustavo F.; Lo Fiego, Marcos J.; Lockhart, Maria T.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 24 p. 2578 - 2585
