in melt placing of mixt. of Pb with SnF2 (molar ratio SnF2:Pb=2.36) in Fluoroplast-4 ampule, closing by screwed stopper, exposition for 1.00 h at 240°C; cooling, stirring up in water, collection, drying;
参考文献
Goryacheva; Rakov; Solov'ev
Russian Journal of Inorganic Chemistry, 2001 , vol. 46, # 7 p. 949 - 952
in [3.3.1]nonane Sn sulfide and freshly pptd. Cu heating in nonane in a sealed tube for 40 h at 160°C, liquid fraction decanting off, solid washing with nonane, solvent removing from combined solns.; Me2SnO isolated as Me2SnCl2;
参考文献
Journal of Organometallic Chemistry, , vol. 264, # 1-2 p. 245 - 252
