in neat (no solvent) byproducts: H2; (N2), Schlenk techniques; heating Sn compd. (200°C) under reducedpressure (1E-3 mm Hg) for 6 h or sealing Sn compd. under reduced pressu re (5E-1 mm Hg) with heating (200°C) for 4 h; isolation of crystals, NMR;
参考文献
Canadian Journal of Chemistry, , vol. 88, # 10 p. 1046 - 1052
in [3.3.1]nonane a mixt. of Sn sulfide and freshly pptd. Cu heating in nonane in a sealed evacuated tube for 40 h at 160°C, liquid product decanting off,solid washing with nonane, solvent removing from combined solns. at 30°C/1 torr; purified by distillation in vacuo;
参考文献
Journal of Organometallic Chemistry, , vol. 264, # 1-2 p. 245 - 252
