THF in tetrahydrofuran absence of air; stirring (room temp., 30 h); filtration off of YbCl2(THF)2 and Sn, evapn. (vac.), washing (hexane), recrystn. (THF);
参考文献
Journal of Organometallic Chemistry, , vol. 436, # 3 p. 299 - 311
NdI2; THF in tetrahydrofuran Me3SnCl in THF added under stirring at -60°C to NdI2 in THF; warmed to room temp.; stirred for 30 min; filtered off; dried; dissolved in water again; analyzed by GLC;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 633, # 2 p. 256 - 260
in ethylene glycol dimethyl ether Irradiation (UV/VIS); under Ar; mole ratio NaBPh4 : SnCl2 = 2 : 1; irradn. (254 nm) for 8 h gave deposition of Sn; deposit sepd., washed with acetone and water, and dried in vac. to give pure Sn;
参考文献
Eisch, John J.; Shah, Jamshed H.; Boleslawski, Marek P.
Journal of Organometallic Chemistry, 1994 , vol. 464, # 1 p. 11 - 22
