prepn. of bronze samples at 1000°C with up to 440 h heating times and annealing studies of 21 d duration at 700°C, Sn content in starting mixt. equiv. to x>0.76;
参考文献
McColm, I. J.; Steadman, R.; Dimbylow, C. S.
Journal of Solid State Chemistry, 1975 , vol. 14, p. 185 - 192
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Gmelin Handbook: W: SVol.B6, 3.3.10.3.4, page 44 - 50
in further solvent(s) byproducts: Ag; To soln. of Ag compd. in EtCN or PrCN twofold or stoich. amt. of elementadded, warmed at 65°C for 16 h; extd. with n-pentane, eluent evapd. in vac. at 0°C, purity checked by elem. anal., mass, (19)F and (13)C NMR spectra;
参考文献
Tyrra, Wieland; Wickleder, Mathias S.
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 8 p. 1841 - 1847
in neat (no solvent) heating in a closed tube at 260°C, 9 days;;
参考文献
Burdon, J.; Coe, P. L.; Fulton, M.
Journal of the Chemical Society, 1965 , p. 2094 - 2096
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Gmelin Handbook: F: PerFHalOrg.4, 4.3.1, page 181 - 183
tetra-(n-butyl)ammonium iodide; zinc in neat (no solvent) Bu4NI, Zn dust and Sn powder heated to 160°C with stirring underN2, alkyl halide added dropwise over 2 h, heated with stirring for further 3 h, cooled slightly; light petroleum added, refluxed for 45 min, cooled, petroleum layer removed by decantation, petroleum distd. off;
参考文献
Nicholson, John W.; Douek, Josephine A.; Collins, John D.
Journal of Organometallic Chemistry, 1982 , vol. 233, # 2 p. 169 - 172
