Stack, W. F.; Nash, G. A.; Skinner, H. A.
Transactions of the Faraday Society, 1965 , vol. 61, p. 2122 - 2125
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5, page 41 - 43
in diethyl ether reaction of tin, CH3CH2OCOCH=CH2 and dry HCl in ethyl ether, product mixt extd. by warm CHCl3; purifn. of monoester by fractional recrystn.;
参考文献
Cheng, Hong-Shing; Hwang, Tsai-Lih; Liu, Chao-Shiuan
Journal of Organometallic Chemistry, 1983 , vol. 254, # 1 p. 43 - 52
in diethyl ether reaction of tin, CH3CH2CH2OCOCH=CH2 and dry HCl in ethyl ether, productmixt extd. by warm CHCl3; purifn. of monoester by fractional recrystn.;
参考文献
Cheng, Hong-Shing; Hwang, Tsai-Lih; Liu, Chao-Shiuan
Journal of Organometallic Chemistry, 1983 , vol. 254, # 1 p. 43 - 52
in ethylene glycol dimethyl ether refluxing for 10 h under N2; detd. by NMR spectrum;
参考文献
Burley, Joseph W.; Hutton, Ronald E.; Jolley, Michael R.J.; Groenenboom, Cornelis J.
Journal of Organometallic Chemistry, 1983 , vol. 251, # 2 p. 189 - 202
in diethyl ether reaction of tin, CH3OCOCH=CH2 and dry HCl in ethyl ether, product mixt extd. by warm CHCl3; purifn. of monoester by fractional recrystn.;
参考文献
Cheng, Hong-Shing; Hwang, Tsai-Lih; Liu, Chao-Shiuan
Journal of Organometallic Chemistry, 1983 , vol. 254, # 1 p. 43 - 52
