反应条件
in neat (no solvent) High Pressure; TiO2 and Mg were heated at 750°C for 5 h under autogenic pressure; react. mixt was gradually cooled to room. temp. for 5 h, MgO was removedby aq. AcOH for 1 day, ppt. was centrifugated, washed with water and Et OH, and dried, washe with formic acid for 2 days, washed and dried;
参考文献
Inorganic Chemistry, , vol. 48, # 15 p. 7066 - 7069
