反应条件
in methanol Electrochem. Process; anodic oxidn. of W in refluxing methanol with LiCl as electrolyte at total 50 V, 150 mA (as in: Seisenbaeva, G. A.; Werndrup, P.; Kloo, L.; Kessler, V. G. Inorg. Chem. 2001, 40, 3815 and Kessler, V. G. etal., J. Chem. Soc., Dalton Trans. 1998, 21); recrystn. (hexane);
参考文献
Pol; Kessler; Seisenbaeva; Solovyov; Gedanken
Inorganic Chemistry, 2005 , vol. 44, # 26 p. 9938 - 9945
