反应条件
ammonia; hydrogen in H2O byproducts: water, nitrogen monoxide, dinitrogen oxide; mixing of (NH4)10W12O41*nH2O in aq. soln. of Cu(NO3)2*3H2O; heating to 90-100°C for 6 h with addn. soln. NH3 and H2O, evapn. (air), calcination at 520°C for 2 h (air), milling, heating in H2 at 400°C for 0.5 h + at 750°C 1.5h; monitoring by XRD;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 55, # 2 p. 167 - 173
