in neat (no solvent) sample heating in TG or DTA apparatus at 10 K/min in static or dynamic air (30 ml/min) in temp. range 25-900°C (intermediate formation intemp. range of 120-180°C); TG, DTA;
in solid electric discharge assisted ball milling; powders mixed; pre-mixed in ball mill for 1 h under Ar; then subjected to ball milling with electric discharge for 5 min; detd. by XRD;
参考文献
Journal of Alloys and Compounds, , vol. 467, # 1-2 p. 477 - 484
