in neat (no solvent) under Ar; powders of BaN2, BaCl2 and BaBr2 (molar ratio 10:2:3) mixed; pelletized; wrapped in Mo foil liner; placed in stainless steel crucible;fired at 998 K for 5 d; cooled slowly (20 K/h); opened in N2 filled glovebox; detd. by X-ray powder diffraction;
Annalen der Physik (Weinheim, Germany), , vol. 32, p. 370
Philosophical Transactions of the Royal Society of London, , p. 336
Ba: MVol., 2.1, page 32 - 37
→
反应条件
in neat (no solvent) under Ar; powders of BaN2, BaCl2 and BaBr2 (molar ratio 10:1:4) mixed; pelletized; wrapped in Mo foil liner; placed in stainless steel crucible;fired at 998 K for 5 d; cooled slowly (20 K/h); opened in N2 filled glovebox; detd. by X-ray powder diffraction;
