Al in neat (no solvent) stoich. amt. of metal, Al and I2 were mixed in a glass-ampoule, chemicaltransport with Al2I6, E5 Pa pressure, ampoule was tempered at 250 .degr ee.C for 3 days, temp. gradient was 350/250 °C, 10 days;
参考文献
Schiefenhoevel; Binnewies; Janetzko; Jug
Zeitschrift fur Anorganische und Allgemeine Chemie, 2001 , vol. 627, # 7 p. 1513 - 1517
in gas static metal vapour atom reactor (according to V. Graves and J. Lagowski, Inorg. Chem., 15 (1976) 577); not isolated, detd. by MAS spectroscopy;
参考文献
Ssekaalo, H.; Lagowski, J. J.; Seymour, C. M.
Inorganica Chimica Acta, 1991 , vol. 183, p. 91 - 96
in gas static metal vapour atom reactor (according to V. Graves and J. Lagowski, Inorg. Chem., 15 (1976) 577); not isolated, detd. by MAS spectroscopy;
参考文献
Ssekaalo, H.; Lagowski, J. J.; Seymour, C. M.
Inorganica Chimica Acta, 1991 , vol. 183, p. 91 - 96
in gas static metal vapour atom reactor (according to V. Graves and J. Lagowski, Inorg. Chem., 15 (1976) 577); not isolated, detd. by MAS spectroscopy;
参考文献
Ssekaalo, H.; Lagowski, J. J.; Seymour, C. M.
Inorganica Chimica Acta, 1991 , vol. 183, p. 91 - 96
