in dichloromethane Electrolysis; controlled-potential electrolysis at Hg electrode in CH2Cl2 at 22°C; electrochemical and spectrophotometrical monitoring; Hg complex identified by comparison with authentic sample;
in dichloromethane Electrolysis; controlled-potential electrolysis at Hg electrode in CH2Cl2 at 22°C; electrochemical and spectrophotometrical monitoring; Hg complex identified by comparison with authentic sample;
in dichloromethane Electrolysis; controlled-potential electrolysis at Hg electrode in CH2Cl2 at 22°C; electrochemical and spectrophotometrical monitoring; Hg complex identified by comparison with authentic sample;
in deuterated toluene using sealed high vac. systems; in NMR tube; Co complex cooled in liq. N2 (77 K); toluene-d8 and AlMe3 (4 equiv.) added; stored at room temp. for 1 d; not isolated; detd. by ESR spectra;