反应条件
in diethyl ether under Ar atm. to soln. Ga complex in Et2O LiP(SiMe3)2*DME in Et2O (1:2) was added at -78°C over 5 min, soln. was warmed to room temp. andstirred overnight; volatiles were emoved in vacuo, residue was extd. with hexane, filtered,concd., and cooled to -30°C overnight; elem. anal.;
参考文献
Antcllff, Karen L.; Baker, Robert J.; Jones, Cameron; Murphy, Damien M.; Rose, Richard P.
Inorganic Chemistry, 2005 , vol. 44, # 6 p. 2098 - 2105
