反应条件
in neat (no solvent) preaparation of GeCl from very pure Ge and Cl2 at 300-350 °C in special app.;; distillation in N2-stream on Hg, shaking, fractional distillation of GeCl4;;
参考文献
Dennis, L. M.; Hance, F. E.
Z. Anorg. Chem., 1922 , vol. 122, p. 272 - 272
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Dennis, L. M.; Hance, F. E.
Journal of the American Chemical Society, 1922 , vol. 44, p. 304 - 304
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Laubengayer, A. W.; Tabern, D. L.
Journal of Physical Chemistry, 1926 , vol. 30, p. 1047 - 1047
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Gmelin Handbook: Ge: MVol., 13, page 40 - 42